https://nesgwiki.chem.buffalo.edu/index.php?action=history&feed=atom&title=Full_probefile_calibration 2026-04-19T01:51:50Z Revision history for this page on the wiki MediaWiki 1.38.2 https://nesgwiki.chem.buffalo.edu/index.php?title=Full_probefile_calibration&diff=3288&oldid=prev 2009-12-15T15:53:42Z

<p></p> <table style="background-color: #fff; color: #202122;" data-mw="interface"> <col class="diff-marker" /> <col class="diff-content" /> <col class="diff-marker" /> <col class="diff-content" /> <tr class="diff-title" lang="en"> <td colspan="2" style="background-color: #fff; color: #202122; text-align: center;">← Older revision</td> <td colspan="2" style="background-color: #fff; color: #202122; text-align: center;">Revision as of 15:53, 15 December 2009</td> </tr><tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l1">Line 1:</td> <td colspan="2" class="diff-lineno">Line 1:</td></tr> <tr><td class="diff-marker" data-marker="−"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>== Full Probefile Calibration ==</div></td><td class="diff-marker" data-marker="+"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>== Full Probefile Calibration <ins style="font-weight: bold; text-decoration: none;"> </ins>==</div></td></tr> <tr><td class="diff-marker"></td><td style="background-color: #f8f9fa; color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><br/></td><td class="diff-marker"></td><td style="background-color: #f8f9fa; color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><br/></td></tr> <tr><td class="diff-marker" data-marker="−"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>This procedure is similar to [[NESG:AutomatedNMRParametersOptimization|Automated Pulse Width Calibration]], but the number of parameters to be optimized is much larger an the required time is much longer. Full calibration is usually needed only after hardware upgrades, e.g. probe or amplifiers.</div></td><td class="diff-marker" data-marker="+"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>This procedure is similar to [[NESG:AutomatedNMRParametersOptimization|Automated Pulse Width Calibration]], but the number of parameters to be optimized is much larger an the required time is much longer. Full calibration is usually needed only after hardware upgrades, e.g. probe or amplifiers.  </div></td></tr> <tr><td class="diff-marker"></td><td style="background-color: #f8f9fa; color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><br/></td><td class="diff-marker"></td><td style="background-color: #f8f9fa; color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><br/></td></tr> <tr><td class="diff-marker" data-marker="−"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div># Insert a concentrated NC-labeled sample of a small protein, preferably in a Varian shigemi with proper filling height. Perform tuning/matching, lock and shim the sample.</div></td><td class="diff-marker" data-marker="+"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>#Insert a concentrated NC-labeled sample of a small protein, preferably in a Varian shigemi with proper filling height. Perform tuning/matching, lock and shim the sample.  </div></td></tr> <tr><td class="diff-marker" data-marker="−"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div># Load the &lt;tt&gt;ghn_co&lt;/tt&gt; dataset and set the desired parameters - type &lt;tt&gt;man('BioPacklist')&lt;/tt&gt; for a list.</div></td><td class="diff-marker" data-marker="+"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>#Load the &lt;tt&gt;ghn_co&lt;/tt&gt; dataset and set the desired parameters - type &lt;tt&gt;man('BioPacklist')&lt;/tt&gt; for a list.  </div></td></tr> <tr><td class="diff-marker" data-marker="−"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div># To start Autocalibration go to '''Setup''' -<del style="font-weight: bold; text-decoration: none;">&gt; </del>'''Calibrations''' and select '''Full, using probefile values''' or '''Full, But Use Current 1H Offset and pw'''</div></td><td class="diff-marker" data-marker="+"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>#To start Autocalibration go to '''Setup''' -<ins style="font-weight: bold; text-decoration: none;">&amp;gt; </ins>'''Calibrations''' and select '''Full, using probefile values''' or '''Full, But Use Current 1H Offset and pw'''</div></td></tr> <tr><td class="diff-marker"></td><td style="background-color: #f8f9fa; color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><br/></td><td class="diff-marker"></td><td style="background-color: #f8f9fa; color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #eaecf0; vertical-align: top; white-space: pre-wrap;"><br/></td></tr> <tr><td class="diff-marker" data-marker="−"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div> </div></td><td class="diff-marker" data-marker="+"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div><ins style="font-weight: bold; text-decoration: none;">&lt;br&gt; </ins>-- Main.AlexEletski - 14 Mar 2008</div></td></tr> <tr><td class="diff-marker" data-marker="−"></td><td style="color: #202122; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>-- Main.AlexEletski - 14 Mar 2008</div></td><td colspan="2" class="diff-side-added"></td></tr> </table>

Aringh https://nesgwiki.chem.buffalo.edu/index.php?title=Full_probefile_calibration&diff=2442&oldid=prev 2009-11-30T19:33:21Z

<p>moved <a href="/index.php/NESG:FullProbeFileCalibration" class="mw-redirect" title="NESG:FullProbeFileCalibration">NESG:FullProbeFileCalibration</a> to <a href="/index.php/Full_probefile_calibration" title="Full probefile calibration">Full probefile calibration</a></p> <table style="background-color: #fff; color: #202122;" data-mw="interface"> <tr class="diff-title" lang="en"> <td colspan="1" style="background-color: #fff; color: #202122; text-align: center;">← Older revision</td> <td colspan="1" style="background-color: #fff; color: #202122; text-align: center;">Revision as of 19:33, 30 November 2009</td> </tr><tr><td colspan="2" class="diff-notice" lang="en"><div class="mw-diff-empty">(No difference)</div> </td></tr></table>

Alex https://nesgwiki.chem.buffalo.edu/index.php?title=Full_probefile_calibration&diff=99&oldid=prev 2009-10-08T15:00:02Z

<p>Created page with &#039;== Full Probefile Calibration == This procedure is similar to <a href="/index.php/NESG:AutomatedNMRParametersOptimization" title="NESG:AutomatedNMRParametersOptimization">Automated Pulse Width Calibration</a>, but the number of parameters to be o…&#039;</p> <p><b>New page</b></p><div>== Full Probefile Calibration ==<br /> <br /> This procedure is similar to [[NESG:AutomatedNMRParametersOptimization|Automated Pulse Width Calibration]], but the number of parameters to be optimized is much larger an the required time is much longer. Full calibration is usually needed only after hardware upgrades, e.g. probe or amplifiers.<br /> <br /> # Insert a concentrated NC-labeled sample of a small protein, preferably in a Varian shigemi with proper filling height. Perform tuning/matching, lock and shim the sample.<br /> # Load the &lt;tt&gt;ghn_co&lt;/tt&gt; dataset and set the desired parameters - type &lt;tt&gt;man('BioPacklist')&lt;/tt&gt; for a list.<br /> # To start Autocalibration go to '''Setup''' -&gt; '''Calibrations''' and select '''Full, using probefile values''' or '''Full, But Use Current 1H Offset and pw'''<br /> <br /> <br /> -- Main.AlexEletski - 14 Mar 2008</div>

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