https://nesgwiki.chem.buffalo.edu/index.php?action=history&feed=atom&title=NMR_experiment_setup_scripts_for_VNMRJ 2026-04-13T00:17:36Z Revision history for this page on the wiki MediaWiki 1.38.2 https://nesgwiki.chem.buffalo.edu/index.php?title=NMR_experiment_setup_scripts_for_VNMRJ&diff=2350&oldid=prev 2009-11-29T23:36:05Z

<p>Created page with &#039;2D [&lt;sup&gt;15&lt;/sup&gt;N,&lt;sup&gt;1&lt;/sup&gt;H] HSQC *HTP_NHSQC_long - 256 complex points in t&lt;sub&gt;1&lt;/sub&gt;, 8 scans, 32 dummy scans *HTP_NHSQC_short - 60 ms t&lt;sub&gt;1,max&lt;/sub&gt;, 4 scans *HTP…&#039;</p> <p><b>New page</b></p><div>2D [&lt;sup&gt;15&lt;/sup&gt;N,&lt;sup&gt;1&lt;/sup&gt;H] HSQC <br /> <br /> *HTP_NHSQC_long - 256 complex points in t&lt;sub&gt;1&lt;/sub&gt;, 8 scans, 32 dummy scans <br /> *HTP_NHSQC_short - 60 ms t&lt;sub&gt;1,max&lt;/sub&gt;, 4 scans <br /> *HTP_NHSQC_wide - 40 ms t&lt;sub&gt;1,max&lt;/sub&gt;, 4 scans, &lt;sup&gt;15&lt;/sup&gt;N spectral width 3 times the probefile value<br /> <br /> &lt;br&gt; <br /> <br /> 2D [&lt;sup&gt;13&lt;/sup&gt;C,&lt;sup&gt;1&lt;/sup&gt;H] HSQC <br /> <br /> *HTP_CaliHSQC - gradient/sensitivy enhanced, &lt;sup&gt;13&lt;/sup&gt;C spectral width 80 ppm, 7 ms t&lt;sub&gt;1,max&lt;/sub&gt;, 4 scans <br /> *HTP_CaroHSQC - gradient/sensitivy enhanced, &lt;sup&gt;13&lt;/sup&gt;C spectral width 40 ppm, 5 ms t&lt;sub&gt;1,max&lt;/sub&gt;, 8 scans <br /> *HTP_ctCaliHSQC - gradient/sensitivy enhanced, &lt;sup&gt;13&lt;/sup&gt;C spectral width 80 ppm, 27 ms constant-time delay <br /> *HTP_ctCaroHSQC - gradient/sensitivy enhanced, &lt;sup&gt;13&lt;/sup&gt;C spectral width 40 ppm, 16 ms constant-time delay <br /> *gChsqc_methyl - 28 ms constant-time delay, optimized for methyl groups&lt;br&gt;<br /> <br /> &lt;br&gt; <br /> <br /> 3D Triple-resonance <br /> <br /> *HTP_HNCO_3D - &lt;sup&gt;13&lt;/sup&gt;C spectral width 20 ppm, 7 ms t&lt;sub&gt;1,max&lt;/sub&gt;, ni2 is 32 or max, 2 scans <br /> *HTP_HNCACO_3D - &lt;sup&gt;13&lt;/sup&gt;C spectral width 20 ppm, 7 ms t&lt;sub&gt;1,max&lt;/sub&gt;, ni2 is 32 or max, 2 scans <br /> *HTP_CBCACONH_3D - &lt;sup&gt;13&lt;/sup&gt;C spectral width 80 ppm, 6 ms t&lt;sub&gt;1,max&lt;/sub&gt; or max allowed, ni2 is 32 or max, 2 scans <br /> *HTP_HNCACB_3D - &lt;sup&gt;13&lt;/sup&gt;C spectral width 80 ppm, 6 ms t&lt;sub&gt;1,max&lt;/sub&gt;, ni2 is 32 or max, 2 scans <br /> *HTP_HBHACONH_3D - &lt;sup&gt;1&lt;/sup&gt;H&lt;sup&gt;ab&lt;/sup&gt; spectral width 9 ppm, 15 ms t&lt;sub&gt;1,max&lt;/sub&gt;, ni2 is 32 or max, 2 scans <br /> *HTP_HCCH_COSY_3D - &lt;br&gt; <br /> *HTP_HCCH_TOCSY_3D</div>

Alex