Resonance Assignment/XEASY: Difference between revisions

Latest revision as of 16:21, 5 January 2010

Introduction
Spin system identification
Backbone resonance assignment
1. GFT-based spectra
  1. HNCACAB/CABCA(CO)NH
2. Conventional spectra
  1. HNCACB/CBCA(CO)NH
Side chain resonance assignment
1. Aliphatic
  1. GFT-based spectra
    1. (4,3)D GFT HABCAB(CO)NHN
    2. (4,3)D GFT HCCH
  2. Conventional spectra
    1. HAHB(CO)NH
    2. HCCH-COSY
    3. Simultaneous NOESY
2. Aromatic
3. Additional side chain atoms

@@ Line 1: / Line 1: @@
+#[[XEASY Introduction|Introduction]]
 #[[XEASY Spin system identification|Spin system identification]]
 #Backbone resonance assignment'''<br>'''
@@ Line 5: / Line 6: @@
 ##Conventional spectra
 ###[[HNCACB/CBCA(CO)NH]]
-###HNCA/HN(CO)CA
+#Side chain resonance assignment
-###HNCO/HN(CA)CO
-###NOESY/TOCSY
-#[[XEASY Side Chain Assignment|Side chain resonance assignment]]
 ##Aliphatic
-###GFT NMR spectra
+###GFT-based spectra
 ####[[HA and HB Assignment with GFT in XEASY|(4,3)D GFT HABCAB(CO)NHN]]
 ####[[Side chain assignment with aliphatic (4,3)D HCCH-COSY in XEASY|(4,3)D GFT HCCH]]
@@ Line 16: / Line 14: @@
 ####HAHB(CO)NH
 ####HCCH-COSY
-####HCCH-TOCSY
 ####[[Side chain assignment with CN-NOESY in XEASY|Simultaneous NOESY]]
-####(H)CC-TOCSY-(CO)NH
-####H(CC-TOCSY-CO)NH
 ##[[Aromatic side chain assignment with Aro-HCCH-COSY in XEASY|Aromatic]]
-###GFT-based spectra
+##Additional side chain atoms
-###Conventional spectra
+###[[Trp e1 and d1 assignment with NOESY|Trp e1 NH and d1 CH]]
-##Other
-###Trp e1 NH and d1 CH
 ###[[Met methyl assignment with NOESY|Met e CH3 ]]
 ###[[Amide Side Chain assignment with NOESY|Asn d2 and Gln e2 NH2]]
-#NOESY peak integration