Metabonomics SOP

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NMR

Safety Protocols

Contact information

NMR Safety Rules

Cryogenic liquids

Magnetic materials

Physical contact

Injury reporting

Biosafety

Safety training

Training records

Vaccination

Universal safety precautions and lab safety policies

Injury logs and reporting

Additional documents

Chemical hygiene plan

Exposure control plan

Sample Storage and Preparation

Serum

Urine

Others:Non-biofluids

Pipetting

Labeling of NMR specimens

Data Acquisition

Profiling of serum

Profiling of urine

Profiling of other specimens:Non-biofluids

For Resonance Assignment

Spiking of Metabolites

Data Archiving

Data Processing

Phase Correction

1D PC

2D PC

Baseline Correction

1D BC

2D BC

Peak Alignment: Recursive Segment-wise

Spectral Quality Assessment (FOM)

Operator Certification?

Targeted Profiling--FOM?

Resonance Assignment

Development of Metabolic Models?

Statistics

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